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Automatic Large Antechamber Door Super Purification Glove Box with IoT System

Glove Box

Automatic Large Antechamber Door Super Purification Glove Box with IoT System

Item Number : ST18

Price varies based on specs and customizations


Atmospheric Purity
< 1 ppm H2O & < 1 ppm O2
Main Antechamber
Ø360 × 600 mm (Automatic Vertical-Lift Door)
Control Architecture
Siemens PLC Touchscreen with Cloud IoT Integration
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Product Overview

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This super purification glove box provides an ultra-clean, controlled inert gas environment tailored specifically for moisture- and oxygen-sensitive scientific research and industrial prototyping. Featuring an integrated closed-loop gas purification column and automated atmospheric management, the system maintains strict purity thresholds below 1 ppm moisture and oxygen levels. By pairing robust 304 stainless steel construction with automated vertical-lift antechamber access and smart cloud-connected IoT architecture, this equipment eliminates contamination risks while significantly streamlining material loading workflows.

Engineered primarily for academic universities, national laboratories, and high-tech research institutions, the system serves as a foundational platform for lithium-ion and solid-state battery fabrication, organometallic synthesis, perovskite solar cell development, and specialized metallurgy. The integrated IoT system empowers laboratory managers and researchers with full remote visibility, real-time operating telemetry, automated maintenance logs, and multi-device coordination, allowing continuous experiments to proceed without requiring constant physical presence at the workstation.

Built to withstand continuous, long-term laboratory operations, the enclosure integrates premium electro-pneumatic valves, high-capacity circulating blowers, and precision gas sensors to ensure steady baseline containment. Whether configured with nitrogen, argon, or helium working gases, this system delivers uncompromising hermetic integrity, dependable vacuum integrity, and fail-safe overpressure protection to safeguard hazardous samples, valuable compounds, and operational personnel in rigorous research environments.

Key Features

  • Sub-PPM Purification Capability: High-efficiency single purification column packed with 5 kg of copper catalyst and 5 kg of molecular sieve achieves and sustains moisture and oxygen levels below 1 ppm, ensuring zero oxidation or hydrolysis during critical synthesis.
  • Intelligent IoT Connectivity: Integrated IoT smart system enables remote mobile control, centralized multi-device fleet management, real-time status synchronization, cloud-based telemetry reports, automatic fault diagnostics, and immediate mobile push alerts for anomalous parameters.
  • Automated Vertical-Lift Large Antechamber: Motorized anodized aluminum vertical-lift door eliminates the swing radius of traditional hinged doors, streamlining high-throughput sample loading while reducing seal wear and mechanical stress on the vacuum chamber.
  • Industrial Siemens PLC Touchscreen Control: Intuitive human-machine interface automates gas circulation, pressure balancing, regeneration cycles, and system self-diagnostics with password-protected multi-level user access.
  • Automated Pressure and Foot-Pedal Regulation: Programmable working chamber pressure settings within ±15 mbar with automatic overpressure protection triggered beyond ±16 mbar, complemented by hands-free foot-pedal pressure adjustments during active glove handling.
  • High-Capacity Closed-Loop Gas Circulation: Integrated circulating blower delivers standard circulation rates of 90 m³/h (upgradeable to 145 m³/h or 180 m³/h) to quickly scrub contaminants following antechamber purge cycles and sample introductions.
  • Automated Regenerative Purification: Fully automated, PLC-controlled thermal regeneration sequence utilizing forming gas (5% to 10% H2 balance inert gas) restores catalyst beds to peak chemical reactivity without requiring manual handling or dismantling.
  • Heavy-Duty Hygienic Stainless Enclosure: Fabricated from 3 mm thick 304 stainless steel with an interior oil-film brushed finish for easy wipe-down decontamination and an exterior mirror polish for enhanced chemical resistance and cleanroom compatibility.
  • Dual Antechamber Architecture: Equipped with both an automated large cylindrical antechamber for bulk equipment transfer and a manual mini antechamber for rapid, low-volume loading of tools, vials, and small reagents without disturbing main chamber equilibrium.
  • Ultra-Fine 0.3 μm In-Line Particulate Filtration: Dual gas inlet and outlet filters prevent catalyst dust, fine powders, and aerosolized particulates from contaminating sensitive experimental substrates or damaging downstream valves.

Applications

Application Description Key Benefit
Solid-State Battery Assembly Handling reactive metallic lithium anodes, solid electrolytes (sulfides/oxides), and moisture-sensitive pouch cell stackings. Prevents passivation and side reactions by maintaining <1 ppm moisture and oxygen during cell assembly.
Perovskite Photovoltaic Research Spin-coating, thermal evaporation, and encapsulation of halide perovskite precursors and active layers. Eliminates rapid environmental degradation, ensuring maximum power conversion efficiency and film reproducibility.
Air-Sensitive Organometallic Chemistry Manipulation, storage, and catalysis of pyrophoric ligands, Grignard reagents, and low-valent transition metal complexes. Eliminates flammable hazard risks while preventing premature catalyst poisoning and compound degradation.
OLED & Microelectronics Encapsulation Deposition and packaging of organic semiconductor materials, conductive inks, and hygroscopic transport layers. Extends device operational lifespan by guaranteeing an ultra-pure, moisture-free sealing environment.
3D Printing Powder Processing Handling, sieving, and recovery of reactive spherical titanium, aluminum, and nickel superalloy powders. Prevents powder oxidation, batch contamination, and dangerous dust ignition during powder handling.
Supercapacitor & Energy Storage R&D Synthesis of high-surface-area porous carbon matrices and moisture-sensitive non-aqueous electrolytes. Guarantees exact electrochemical window stability without trace water contamination causing parasitic gas evolution.

Technical Specifications

Subsystem / Assembly Parameter Specification (ST18)
Model Configuration Base Identification ST18
Chamber Body Internal Dimensions (L × D × H) 1200 mm × 750 mm × 900 mm
Structural Material 304 Stainless Steel, 3.0 mm Thickness
Internal Surface Treatment Oil-film brushed hygienic finish
External Surface Treatment Mirror-polished finish
Viewing Window Slanted 8.0 mm tempered safety glass
Glove Ports POM / Aluminum Alloy with O-ring hermetic seal
Gloves Butyl rubber, 0.4 mm thickness, 7" or 8" port diameter
Internal Shelving 2-tier height-adjustable stainless steel shelf
Chamber Illumination Internal hood-mounted LED lighting system
Utility Feedthroughs Standard DN40KF blank ports + 1 × 220V internal power interface
Particulate Filtration Dual 0.3 μm gas inlet and outlet HEPA-grade filters
Purification Unit Purification Column Configuration Single-column regenerative purifier
Target Gas Removal Purity H2O < 1 ppm, O2 < 1 ppm
Purification Reactants 5 kg Copper Catalyst + 5 kg Molecular Sieve
Chemical Adsorption Capacity Deoxygenation: 60 L O2; Dehydration: 2.0 kg H2O
Compatible Working Gases Nitrogen (N2), Argon (Ar), Helium (He)
Circulation Blower Flow Rate 90 m³/h integrated blower (Optional: 145 m³/h, 180 m³/h)
Regeneration Cycle Control Fully automated PLC sequence
Regeneration Gas Requirement Working gas blended with 5% to 10% Hydrogen (H2)
Main Angle Valves DN40KF electro-pneumatic angle valves
Process Control Valves Integrated solenoid manifold assembly
Main Large Antechamber Chamber Dimensions Diameter 360 mm × Length 600 mm (Optional: Diameter 400 mm)
Material & Finish 304 Stainless Steel (Internal brushed, external mirror polish)
Door Construction 10 mm anodized aluminum vertical-lift automated door mechanism
Material Handling Stainless steel sliding material tray
Operational Control Automatic PLC-managed evacuation and refill cycle
Pressure Display Integrated analog differential pressure gauge
Secondary Mini Antechamber Chamber Dimensions Diameter 150 mm × Length 300 mm (Optional: Diameter 100 mm)
Material & Finish 304 Stainless Steel (Internal brushed, external mirror polish)
Door Operation Dual manual hinged doors with tight-seal clamping
Pressure Display Integrated analog vacuum gauge
Control & IoT System Central Controller Siemens PLC with high-resolution touchscreen HMI
Pressure Regulation Range User-configurable within ±15 mbar
Overpressure Protection Automatic active protection triggered at ±16 mbar
Hands-Free Control Bi-directional foot pedal for chamber pressure adjustment
IoT Network Functions Mobile remote control, multi-device management, real-time data sync
Data & Diagnostics Automated data report logging, historical query, remote diagnostic repair
System Redundancy Auto-diagnostic self-checks with power-failure auto-restart
Analytical Sensors & Pump Oxygen Sensor Measurement Range 0 to 1000 ppm
Dew Point / Moisture Sensor Range 0 to 500 ppm
Vacuum Pump Specifications Rotary vane pump (8 m³/h, 12 m³/h, or 16 m³/h options)
Pump Protection Features Integrated exhaust oil-mist filter and gas ballast control

Why Choose This Product

  • Industrial-Grade Vacuum Engineering: Built with 3 mm heavy-gauge 304 stainless steel and CNC-machined DN40KF ports, this workstation provides zero-leak performance and structural rigidity under continuous deep-vacuum transfer cycles.
  • Connected Laboratory Management: The integrated cloud IoT architecture transitions your laboratory into an intelligent, connected workspace—enabling proactive equipment maintenance, real-time mobile parameter tracking, and automated historical data compliance reporting.
  • Ergonomic & Space-Saving Automation: The automated vertical-lift large antechamber reduces operator fatigue, avoids workstation clutter associated with traditional swing-door mechanisms, and guarantees repeatable sealing pressure across thousands of operation cycles.
  • Complete Analytical Transparency: Integrated solid-state trace moisture and oxygen analyzers provide immediate, accurate feedback, ensuring sensitive materials are only handled when the operating environment strictly meets sub-ppm criteria.

Contact our technical engineering team today to receive a detailed quotation, discuss custom dimensional requests, or configure specialized feedthroughs for your advanced research facility.

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Product Datasheet

Automatic Large Antechamber Door Super Purification Glove Box with IoT System

Category Catalog

Glove Box


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