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Single Station Touchscreen Glovebox Inert Atmosphere Purification System

Glove Box

Single Station Touchscreen Glovebox Inert Atmosphere Purification System

Item Number : ST14

Price varies based on specs and customizations


Atmosphere Purity Level
< 1 ppm H₂O & < 1 ppm O₂
Internal Box Dimensions
1220 mm (L) × 750 mm (D) × 900 mm (H)
Circulation Blower Flow Rate
90 m³/h with Variable Frequency Drive (VFD)
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Product Overview

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This single station touchscreen glovebox is an integrated inert atmosphere containment system engineered specifically for sensitive electrochemical synthesis, advanced materials preparation, and moisture-critical assembly operations. Featuring an autonomous single-column gas purification system, the equipment continuously scrubs recirculating inert gas to maintain an ultra-pure environment with moisture and oxygen concentrations below 1 ppm. Its single-sided operational layout combines ergonomic visibility with a heavy-duty hermetic enclosure, delivering complete contamination control for next-generation research.

Designed primarily for solid-state battery R&D, sulfide electrolyte formulation, and organometallic synthesis, this system addresses the acute safety and purity demands of reactive chemical processing. The platform integrates a specialized hydrogen sulfide (H₂S) scrubbing column alongside hydrofluoric acid (HF) removal traps, protecting both the core purification catalyst and operating personnel from volatile byproducts during active material handling and cell assembly workflows.

Built on a rigid 304 stainless steel architecture, the workstation incorporates an advanced Siemens PLC interface, dual stainless steel antechambers, a variable-frequency circulation blower, and automated chamber pressure balancing. Whether running continuous baseline experiments or handling demanding synthesis cycles, this equipment ensures repeatable atmospheric purity, robust chemical resistance, and long-term operational dependability under rigorous laboratory conditions.

Key Features

  • Ultra-Pure Working Atmosphere: Closed-loop gas purification maintains moisture ($H_2O$) and oxygen ($O_2$) levels at less than 1 ppm under standard inert conditions ($20^\circ\text{C}$, 1 atm, 99.999% inert gas supply) with an exceptional leak rate of $\le 0.05\text{ vol}%/\text{h}$.
  • Dedicated Sulfide & Acid Vapor Scrubbing: Integrated chemical absorption systems—including a dedicated H₂S trapping column and HF scrubber—actively remove volatile reaction byproducts before they can degrade the main purification catalyst or contaminate the internal chamber.
  • Siemens PLC & Touchscreen Automation: High-resolution interface centralizes system self-diagnostics, automated chamber purging, power-off auto-restart capabilities, real-time parameter logging, and password-protected administrative controls.
  • Dual Stainless Steel Antechambers: Equipped with a large cylindrical chamber ($Ø360\text{ mm} \times 600\text{ mm}$) featuring a vertical-lift anodized door with a sliding tray, plus a compact chamber ($Ø150\text{ mm} \times 300\text{ mm}$) for rapid, low-consumption sample introduction.
  • High-Capacity Closed-Loop Purification: Houses 5 kg of high-activity copper catalyst (60 L $O_2$ capacity) and 5 kg of precision molecular sieve (2 kg $H_2O$ capacity) driven by a 90 $m^3/h$ variable-frequency blower.
  • Automated Catalyst Regeneration: Microprocessor-managed thermal regeneration cycle restores moisture and oxygen absorption beds automatically using standard forming gas mixtures (5–10% $H_2$ in inert carrier gas).
  • Precision Dynamic Pressure Control: Programmable system regulates chamber pressure within a user-defined $\pm 15\text{ mbar}$ envelope, backed by automatic $\pm 16\text{ mbar}$ over/underpressure safety tripping and hands-free foot pedal adjustment.
  • Advanced Analytical Instrumentation: High-accuracy P₂O₅ moisture analyzer ($0\text{--}500\text{ ppm}$, cleanable and reusable probe) and electrochemical oxygen sensor ($0\text{--}1000\text{ ppm}$) deliver responsive $0.1\text{ ppm}$ resolution.
  • Heavy-Duty Ergonomic Enclosure: Constructed from 3 mm acid-resistant 304 stainless steel with a brushed interior, paired with an 8 mm inclined tempered safety glass window and leak-tight aluminum alloy glove ports with butyl rubber gloves.

Applications

Application Description Key Benefit
Solid-State Battery Assembly Enclosing sulfide- and halide-based solid electrolyte synthesis, pellet pressing, and solid-state cell stacking. Prevents moisture-triggered hydrolysis and toxic gas release while maintaining high ionic conductivity in assembled cells.
Sulfide Electrolyte Synthesis Formulating, milling, and annealing volatile sulfide precursor materials ($Li_2S$, $P_2S_5$) with inline H₂S absorption. Traps corrosive sulfurous volatiles to protect internal hardware, catalyst beds, and laboratory operators.
Lithium & Sodium Metal Processing Handling, cutting, laminating, and encapsulating highly reactive alkali metal anodes and thin foils. Eliminates oxidation and passivation layers, ensuring uniform interfacial contact and prolonged cycle life.
Organometallic & Catalyst Chemistry Synthesizing air-sensitive coordination compounds, Grignard reagents, and radical polymerization catalysts. Delivers a consistent sub-ppm inert environment that eliminates moisture-induced catalyst degradation.
Perovskite & Optoelectronic R&D Spin-coating, thermal annealing, and packaging organic-inorganic hybrid perovskite precursor films. Protects moisture-labile halides from degradation, ensuring high film uniformity and reproducible device efficiency.
Hazardous Powder Containment Controlled dispensing, weighing, and mechanical transfer of reactive, toxic, or hygroscopic nanomaterials. Interlocked dual antechambers and sealed HEPA filtration prevent environmental release and external contamination.

Technical Specifications

System Component Parameter / Specification Engineering Detail (Item Number: ST14)
Model Identifier Model Item Number ST14
Workstation Geometry Workstation Configuration Single station, single-sided operation (2 glove ports)
Internal Dimensions ($L \times D \times H$) $1220\text{ mm} \times 750\text{ mm} \times 900\text{ mm}$
Enclosure Material 304 Stainless Steel, 3.0 mm wall thickness, acid-resistant
Surface Treatment Internal: Brushed stainless finish; External: Powder-coated white
Atmosphere Performance Working Gas Compatibility High-purity Nitrogen ($N_2$), Argon ($Ar$), or Helium ($He$)
Baseline Gas Purity $H_2O < 1\text{ ppm}$, $O_2 < 1\text{ ppm}$ (at $20^\circ\text{C}$, 1 atm, 99.999% inert supply)
Leakage Rate $\le 0.05\text{ vol}%/\text{h}$
Operating Pressure Range User-configurable within $\pm 15\text{ mbar}$; auto-safety trip at $\pm 16\text{ mbar}$
Pressure Adjustment Automated PLC control via solenoid manifold and auxiliary foot pedal
Front Window & Optics Window Construction Inclined ergonomic design, 8.0 mm tempered safety glass
Window Sealing Mechanism Solid continuous O-ring flange structure (vacuum-rated hermetic seal)
Glove Ports High-strength aluminum alloy, dual O-ring seal, 8-inch diameter
Gloves Heavy-duty Butyl rubber, 8-inch (203 mm) cuff diameter, 32-inch (812 mm) length
Illumination High-efficiency external LED lighting fixture mounted above front viewing pane
Gas Purification Unit Column Design Single-column 304 stainless steel regenerative containment vessel
Purification Charge 5.0 kg High-Activity Copper Catalyst; 5.0 kg Molecular Sieve
Removal Capacity Oxygen capacity: 60 L; Moisture capacity: 2.0 kg
Gas Circulation Blower Integrated high-flow blower, $90\text{ m}^3/\text{h}$ throughput with Variable Frequency Drive (VFD)
Regeneration Cycle Fully automated PLC sequence using $N_2/H_2$ or $Ar/H_2$ (5–10% $H_2$) forming gas
Valve Architecture DN40 KF electro-pneumatic main angle valve; 6-valve integrated stainless manifold block
Antechamber Systems Large Antechamber Dimensions Cylindrical, $\text{Diameter } 360\text{ mm} \times \text{Length } 600\text{ mm}$ (Right-hand mount)
Large Chamber Construction 304 Stainless steel body; interior brushed finish, exterior powder-coated white
Large Chamber Doors & Tray Dual 10 mm anodized aluminum doors with vertical-lift mechanism; 304 SS sliding tray
Small Antechamber Dimensions Cylindrical, $\text{Diameter } 150\text{ mm} \times \text{Length } 300\text{ mm}$ (enters box 100 mm)
Small Chamber Construction 304 Stainless steel with dual clamp-action compression doors; 304 SS sliding tray
Antechamber Evacuation/Refill Automated touchscreen solenoid valve control with digital vacuum/pressure readouts
Specialized Scrubber Units Hydrogen Sulfide ($H_2S$) Trap Dimensions: $Ø238\text{ mm} \times 407\text{ mm}$; 3.0 mm 304 SS shell with active adsorbent
$H_2S$ Circuit Integration Direct inline connection to main recirculation loop; includes vacuum-purge capability
Hydrofluoric Acid ($HF$) Trap Dedicated inline chemical neutralization trap for fluoride-containing electrolytes
Analytical Sensors Moisture Analyzer ($H_2O$) Range: $0\text{--}500\text{ ppm}$; Resolution: $0.1\text{ ppm}$; Regenerable/cleanable $P_2O_5$ sensor
Oxygen Analyzer ($O_2$) Range: $0\text{--}1000\text{ ppm}$; Resolution: $0.1\text{ ppm}$; High-selectivity electrochemical cell
Vacuum System Rotary Vacuum Pump Heavy-duty oil-sealed rotary vane pump, $12\text{ m}^3/\text{h}$ displacement rate
Ultimate Vacuum Rating $\le 2 \times 10^{-1}\text{ Pa}$ ($2 \times 10^{-3}\text{ mbar}$)
Vacuum Control Integration Automated PLC pump demand control and manual override mode
Fittings & Internal Utility Gas Filtration Dual $0.3\text{ }\mu\text{m}$ HEPA particulate filters (1 gas inlet / 1 gas outlet)
Spare Utility Interfaces 4 blind feedthrough flanges (DN40 KF) on side/rear panels
Internal Electrical Feedthrough 1 integrated 220V power supply interface
Storage Shelving Integrated 3-tier adjustable stainless steel shelving system
Base Structure Rigid structural steel support stand equipped with heavy-duty leveling casters

Why Choose This Product

  • Targeted Engineering for Sulfide Chemistries: Unlike standard atmosphere enclosures that suffer catalyst poisoning from reactive sulfur vapors, this system features dedicated H₂S and HF traps coupled with automated safety interlocks that safeguard both the purification train and laboratory environment.
  • Zero-Loss Sensor Economics: Equipped with a cleanable, regenerable P₂O₅ moisture sensor, this equipment eliminates the recurring cost of sensor disposal following chemical saturation events, dramatically reducing lifetime operating overhead.
  • Precision Atmosphere Stability: High-capacity purification media beds combined with a variable-frequency $90\text{ m}^3/\text{h}$ circulation loop ensure swift recovery to sub-ppm moisture and oxygen levels after antechamber transfer cycles.
  • Turnkey Integration & Process Flexibility: Outfitted with dual vacuum antechambers, digital pressure regulation, multi-tier shelving, and multiple spare DN40 KF ports, this unit readily adapts to specialized feedthroughs, analytical cabling, and internal processing apparatus.

Contact our technical sales team today to configure your single station glovebox system or request a detailed quotation for your battery R&D facility.

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Product Datasheet

Single Station Touchscreen Glovebox Inert Atmosphere Purification System

Category Catalog

Glove Box


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