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CR2016 In Situ XRD X Ray Analysis Double Sided Window Coin Cell Battery Case

Battery supporting materials

CR2016 In Situ XRD X Ray Analysis Double Sided Window Coin Cell Battery Case

Item Number : FZ08

Price varies based on specs and customizations


Form Factor & Dimensions
CR2016 (20 mm x 1.6 mm)
Window Material & Thickness
Polyimide (Kapton), 0.18 mm
Cathode Coating & Thickness
Aluminum Coating (< 0.01 mm)
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Product Overview

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This specialized coin cell casing is an advanced hardware solution engineered specifically for in-situ and operando X-ray diffraction (XRD) characterization of electrochemical storage materials. Featuring dual-sided optical-grade polyimide (Kapton) transmission windows, the casing allows focused X-ray beams to penetrate directly through both the positive and negative sides of an operational battery cell. By maintaining active electrochemical performance during real-time structural analysis, this system eliminates the artifacts, degradation, and relaxation phenomena traditionally associated with ex-situ post-mortem battery teardowns.

Designed primarily for academic institutions, energy research laboratories, synchrotron facilities, and commercial battery R&D centers, this hardware accommodates advanced studies across lithium-ion, sodium-ion, solid-state, and next-generation battery chemistries. The specialized architecture allows researchers to map crystallographic phase transitions, lattice expansion and contraction, staging phenomena in intercalation compounds, and solid-state reaction kinetics under live charge-discharge conditions.

Manufactured under stringent dimensional and metallurgical tolerances, this cell assembly ensures high repeatability and hermetic integrity across long-duration cycling protocols. A dedicated aluminum coating on the interior of the positive shell provides superior electrochemical passivation, preventing high-voltage parasitic oxidation and electrolyte corrosion. This level of material stability guarantees clean, high-signal-to-noise diffraction patterns while safeguarding delicate laboratory equipment against electrolyte leakage.

Key Features

  • Dual Polyimide (Kapton) Transmission Windows: Integrated with precision-aligned 10 mm diameter optical apertures on both the cathode and anode shells, providing an unhindered beam path for both transmission and reflection XRD geometries with minimal background scattering.
  • Precision-Calibrated 0.18 mm Window Thickness: The polyimide membrane is engineered to a uniform 0.18 mm thickness, delivering an optimal balance between structural rigidity to withstand cell crimping pressures and superior X-ray photon transmittance across standard laboratory and synchrotron wavelengths.
  • Protective Cathode Aluminum Coating: The internal surface of the positive shell features a high-purity aluminum coating with a thickness of less than 0.01 mm, safeguarding the casing against high-potential anodic dissolution and minimizing parasitic side reactions during high-voltage cycling.
  • Standardized CR2016 Dimensional Compatibility: Built to the universally recognized 20 mm diameter and 1.6 mm height profile, the casing integrates smoothly with standard coin cell crimpers, testing fixtures, multi-channel potentiostats, and automated XRD sample stages.
  • Exceptional Hermetic Sealing Reliability: Engineered to maintain structural and atmospheric seals when crimped with compatible sealing gaskets, isolating volatile organic electrolytes and air-sensitive electrode materials from ambient moisture and oxygen over extended testing cycles.
  • Low Background Scattering Interference: The selected polyimide window material exhibits an exceptionally low and predictable amorphous diffraction background, enabling precise deconvolution of subtle crystalline phase peaks and low-intensity superlattice reflections.
  • Standardized Five-Piece Research Packaging: Supplied in convenient 5-set packaging units, each batch undergoing strict quality inspection to ensure consistent shell dimensions, defect-free window adhesion, and uniform aluminum coating distribution.

Applications

Application Description Key Benefit
Operando Phase Transition Tracking Continuous XRD monitoring of cathode and anode crystal structures during galvanostatic and potentiostatic cycling. Captures transient intermediate phases and non-equilibrium structural states in real time without cell disassembly.
Solid-State Battery Interface Characterization High-resolution X-ray penetration through dual windows to observe chemo-mechanical evolution at solid electrolyte-electrode interfaces. Detects interface void formation, interphase layer growth, and structural strain under operational compression.
Synchrotron Radiation Beamline Studies High-flux transmission and grazing-incidence XRD experiments conducted at national synchrotron light sources. Delivers high signal-to-noise data under high-intensity X-ray beams without degrading the polyimide window membrane.
High-Voltage Cathode Degradation Analysis Evaluating phase transitions, oxygen release structural collapse, and transition metal dissolution in high-voltage materials. Aluminum cathode coating prevents current collector corrosion at high potentials (>4.5V vs. Li/Li+), isolating active material mechanics.
Anode Intercalation & Plating Investigations Observing staging mechanisms in graphite, silicon-alloying volume changes, and the onset of dendrite formation on metallic anodes. Allows direct structural differentiation between reversible intercalation compounds and irreversible dead metal deposition.
Fast-Charging Dynamic Phase Mapping Analyzing rapid structural shifts and thermal-structural strain in battery electrodes subjected to high C-rate cycling protocols. Provides clear diffraction peak evolution at high temporal resolution without mechanical failure of the sealed cell casing.

Technical Specifications

Parameter Specification Details (FZ08)
Product Identifier FZ08
Product Classification In-Situ X-Ray Analysis Double-Sided Window Coin Cell Case
Standard Form Factor CR2016 Profile
Casing Outer Dimensions (Diameter x Height) 20.0 mm x 1.6 mm
X-Ray Window Configuration Double-Sided (Cathode Shell & Anode Shell Windows)
Window Aperture Diameter Approximately 10.0 mm
Window Membrane Material High-Purity Polyimide (Kapton) Film
Polyimide Membrane Thickness 0.18 mm
Cathode Surface Treatment High-Purity Aluminum Coating
Cathode Coating Layer Thickness < 0.01 mm (< 10 µm)
Unit Weight (Per Assembly) Approximately 0.25 oz (7.0 g)
Primary Analytical Application In-situ and Operando XRD Crystal Structure & Phase Analysis
Standard Package Quantity 5 complete sets per package

Why Choose This Product

  • Engineered specifically for clean diffraction data: The ultra-uniform 0.18 mm polyimide window material minimizes X-ray beam absorption and produces a flat, low amorphous background, maximizing the clarity of peak resolution for complex crystalline transitions.
  • Robust chemical and electrochemical barrier: Featuring a sub-0.01 mm aluminum protective coating on the positive casing, the assembly resists high-voltage oxidative corrosion, ensuring electrolyte stability and preventing false electrochemical signals.
  • Precision manufacturing and tight tolerances: Standardized CR2016 external dimensions ensure perfect fitment with standard laboratory crimping dies, sample holders, and precision automated XRD alignment stages without requiring custom tooling.
  • Superior seal integrity for volatile systems: Engineered to support standard internal components—including wave springs, spacer discs, and sealing gaskets—maintaining an airtight seal that prevents electrolyte evaporation and contamination during multi-day operando experiments.

For technical assistance, bulk procurement, or specialized configuration inquiries regarding our in-situ battery characterization hardware, contact our specialized engineering team today to request a quotation.

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Product Datasheet

CR2016 In Situ XRD X Ray Analysis Double Sided Window Coin Cell Battery Case

Category Catalog

Battery Supporting Materials


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