Battery supporting materials
CR2016 In Situ XRD X Ray Analysis Double Sided Window Coin Cell Battery Case
Item Number : FZ08
Price varies based on specs and customizations
- Form Factor & Dimensions
- CR2016 (20 mm x 1.6 mm)
- Window Material & Thickness
- Polyimide (Kapton), 0.18 mm
- Cathode Coating & Thickness
- Aluminum Coating (< 0.01 mm)
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Product Overview


This specialized coin cell casing is an advanced hardware solution engineered specifically for in-situ and operando X-ray diffraction (XRD) characterization of electrochemical storage materials. Featuring dual-sided optical-grade polyimide (Kapton) transmission windows, the casing allows focused X-ray beams to penetrate directly through both the positive and negative sides of an operational battery cell. By maintaining active electrochemical performance during real-time structural analysis, this system eliminates the artifacts, degradation, and relaxation phenomena traditionally associated with ex-situ post-mortem battery teardowns.
Designed primarily for academic institutions, energy research laboratories, synchrotron facilities, and commercial battery R&D centers, this hardware accommodates advanced studies across lithium-ion, sodium-ion, solid-state, and next-generation battery chemistries. The specialized architecture allows researchers to map crystallographic phase transitions, lattice expansion and contraction, staging phenomena in intercalation compounds, and solid-state reaction kinetics under live charge-discharge conditions.
Manufactured under stringent dimensional and metallurgical tolerances, this cell assembly ensures high repeatability and hermetic integrity across long-duration cycling protocols. A dedicated aluminum coating on the interior of the positive shell provides superior electrochemical passivation, preventing high-voltage parasitic oxidation and electrolyte corrosion. This level of material stability guarantees clean, high-signal-to-noise diffraction patterns while safeguarding delicate laboratory equipment against electrolyte leakage.
Key Features
- Dual Polyimide (Kapton) Transmission Windows: Integrated with precision-aligned 10 mm diameter optical apertures on both the cathode and anode shells, providing an unhindered beam path for both transmission and reflection XRD geometries with minimal background scattering.
- Precision-Calibrated 0.18 mm Window Thickness: The polyimide membrane is engineered to a uniform 0.18 mm thickness, delivering an optimal balance between structural rigidity to withstand cell crimping pressures and superior X-ray photon transmittance across standard laboratory and synchrotron wavelengths.
- Protective Cathode Aluminum Coating: The internal surface of the positive shell features a high-purity aluminum coating with a thickness of less than 0.01 mm, safeguarding the casing against high-potential anodic dissolution and minimizing parasitic side reactions during high-voltage cycling.
- Standardized CR2016 Dimensional Compatibility: Built to the universally recognized 20 mm diameter and 1.6 mm height profile, the casing integrates smoothly with standard coin cell crimpers, testing fixtures, multi-channel potentiostats, and automated XRD sample stages.
- Exceptional Hermetic Sealing Reliability: Engineered to maintain structural and atmospheric seals when crimped with compatible sealing gaskets, isolating volatile organic electrolytes and air-sensitive electrode materials from ambient moisture and oxygen over extended testing cycles.
- Low Background Scattering Interference: The selected polyimide window material exhibits an exceptionally low and predictable amorphous diffraction background, enabling precise deconvolution of subtle crystalline phase peaks and low-intensity superlattice reflections.
- Standardized Five-Piece Research Packaging: Supplied in convenient 5-set packaging units, each batch undergoing strict quality inspection to ensure consistent shell dimensions, defect-free window adhesion, and uniform aluminum coating distribution.
Applications
| Application | Description | Key Benefit |
|---|---|---|
| Operando Phase Transition Tracking | Continuous XRD monitoring of cathode and anode crystal structures during galvanostatic and potentiostatic cycling. | Captures transient intermediate phases and non-equilibrium structural states in real time without cell disassembly. |
| Solid-State Battery Interface Characterization | High-resolution X-ray penetration through dual windows to observe chemo-mechanical evolution at solid electrolyte-electrode interfaces. | Detects interface void formation, interphase layer growth, and structural strain under operational compression. |
| Synchrotron Radiation Beamline Studies | High-flux transmission and grazing-incidence XRD experiments conducted at national synchrotron light sources. | Delivers high signal-to-noise data under high-intensity X-ray beams without degrading the polyimide window membrane. |
| High-Voltage Cathode Degradation Analysis | Evaluating phase transitions, oxygen release structural collapse, and transition metal dissolution in high-voltage materials. | Aluminum cathode coating prevents current collector corrosion at high potentials (>4.5V vs. Li/Li+), isolating active material mechanics. |
| Anode Intercalation & Plating Investigations | Observing staging mechanisms in graphite, silicon-alloying volume changes, and the onset of dendrite formation on metallic anodes. | Allows direct structural differentiation between reversible intercalation compounds and irreversible dead metal deposition. |
| Fast-Charging Dynamic Phase Mapping | Analyzing rapid structural shifts and thermal-structural strain in battery electrodes subjected to high C-rate cycling protocols. | Provides clear diffraction peak evolution at high temporal resolution without mechanical failure of the sealed cell casing. |
Technical Specifications
| Parameter | Specification Details (FZ08) |
|---|---|
| Product Identifier | FZ08 |
| Product Classification | In-Situ X-Ray Analysis Double-Sided Window Coin Cell Case |
| Standard Form Factor | CR2016 Profile |
| Casing Outer Dimensions (Diameter x Height) | 20.0 mm x 1.6 mm |
| X-Ray Window Configuration | Double-Sided (Cathode Shell & Anode Shell Windows) |
| Window Aperture Diameter | Approximately 10.0 mm |
| Window Membrane Material | High-Purity Polyimide (Kapton) Film |
| Polyimide Membrane Thickness | 0.18 mm |
| Cathode Surface Treatment | High-Purity Aluminum Coating |
| Cathode Coating Layer Thickness | < 0.01 mm (< 10 µm) |
| Unit Weight (Per Assembly) | Approximately 0.25 oz (7.0 g) |
| Primary Analytical Application | In-situ and Operando XRD Crystal Structure & Phase Analysis |
| Standard Package Quantity | 5 complete sets per package |
Why Choose This Product
- Engineered specifically for clean diffraction data: The ultra-uniform 0.18 mm polyimide window material minimizes X-ray beam absorption and produces a flat, low amorphous background, maximizing the clarity of peak resolution for complex crystalline transitions.
- Robust chemical and electrochemical barrier: Featuring a sub-0.01 mm aluminum protective coating on the positive casing, the assembly resists high-voltage oxidative corrosion, ensuring electrolyte stability and preventing false electrochemical signals.
- Precision manufacturing and tight tolerances: Standardized CR2016 external dimensions ensure perfect fitment with standard laboratory crimping dies, sample holders, and precision automated XRD alignment stages without requiring custom tooling.
- Superior seal integrity for volatile systems: Engineered to support standard internal components—including wave springs, spacer discs, and sealing gaskets—maintaining an airtight seal that prevents electrolyte evaporation and contamination during multi-day operando experiments.
For technical assistance, bulk procurement, or specialized configuration inquiries regarding our in-situ battery characterization hardware, contact our specialized engineering team today to request a quotation.
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Product Datasheet
CR2016 In Situ XRD X Ray Analysis Double Sided Window Coin Cell Battery Case
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