Products Cell Assembly & Filling Equipment Glove Box Glove Box Integrated Vacuum Coating System for Advanced Thin Film Deposition
Glove Box Integrated Vacuum Coating System for Advanced Thin Film Deposition

Glove Box

Glove Box Integrated Vacuum Coating System for Advanced Thin Film Deposition

Item Number : ST16

Price varies based on specs and customizations


Base Vacuum Level
≤ 5.0 × 10⁻⁴ Pa
Glove Box Atmosphere Purity
H2O < 1 ppm, O2 < 1 ppm
Deposition Sources
Thermal Evaporation & Magnetron Sputtering (DC/RF)
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Product Overview

Glove Box Integrated Vacuum Coating System for Advanced Thin Film Deposition 1

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This integrated system seamlessly merges a high-vacuum physical vapor deposition chamber with a hermetically sealed, ultra-pure inert atmosphere glove box workstation. Engineered specifically to eliminate the risks of ambient degradation, the platform allows operators to load substrates, deposit delicate organic or inorganic thin films, transfer coated samples, and complete critical encapsulation and characterization steps without ever breaking inert gas containment. By maintaining an ultra-clean environment with sub-ppm oxygen and moisture levels throughout the entire workflow, the equipment guarantees exceptional interface purity and superior device performance.

Designed primarily for cutting-edge energy and optoelectronic research, this integrated solution serves critical roles in the fabrication of perovskite solar cells, organic light-emitting diodes (OLEDs), polymer light-emitting diodes (PLEDs), semiconductor devices, and functional nanomaterials. Academic institutions, industrial R&D laboratories, and pilot-line production facilities rely on this architecture to process moisture-sensitive, air-reactive precursors and organic active layers with absolute repeatability.

Constructed with industrial-grade stainless steel chambers, precision multi-source evaporation assemblies, advanced magnetron sputtering configurations, and high-efficiency closed-loop gas purification systems, the unit delivers steadfast operational stability under demanding research schedules. The rigid mechanical coupling between the vacuum chamber and glove box glove ports prevents vibrational interference, ensuring long-term operational integrity and uncompromised vacuum containment for high-yield thin film synthesis.

Key Features

  • Seamless Glove Box Integration: The deposition chamber mounts directly to the glove box shell via a sealed transfer interface, enabling direct substrate loading, post-coating manipulation, and encapsulation under continuous inert conditions without atmospheric exposure.
  • Ultra-Pure Closed-Loop Gas Purification: Integrated purification columns continuously scrub the glove box atmosphere to maintain H2O and O2 concentrations below 1 ppm, shielding sensitive halide perovskites and organic charge-transport layers from environmental degradation.
  • Multi-Source Thermal Deposition Capabilities: Equipped with independently controlled resistance-heating evaporation sources, shielding cross-talk baffles, and precision power supplies to facilitate layer-by-layer or co-evaporation of organic molecules, metal electrodes, and precursor salts.
  • Multi-Functional Magnetron Sputtering Module: Configurable with balanced and unbalanced DC/RF magnetron sputtering heads to deposit high-density metallic films, transparent conducting oxides, dielectric barriers, magnetic layers, and complex semiconductor alloys.
  • High-Vacuum Pumping System: High-throughput turbomolecular pumping stations backed by chemical-resistant dry scroll pumps achieve deep baseline vacuum levels rapidly, reducing turnaround times while preventing oil backstreaming and substrate contamination.
  • Precision Quartz Crystal Film Thickness Monitoring: Integrated multi-channel quartz crystal microbalances (QCM) deliver real-time deposition rate and thickness tracking with sub-angstrom resolution, ensuring exact stoichiometric control and uniform thickness profiles.
  • Substrate Rotation and Temperature Conditioning: Features motorized substrate rotation for excellent radial film uniformity across large sample areas, paired with programmable radiant heating and cooling stages to tailor thin-film crystallization kinetics.
  • Ergonomic Antechamber and Transfer System: Includes standard large cylindrical and mini antechambers with automated evacuation and refilling cycles to transfer substrates, chemicals, and tooling quickly without disturbing glove box equilibrium.
  • PLC-Driven Touchscreen Control: Centralized programmable logic controller with an intuitive graphical interface manages vacuum cycling, gas regeneration, source power ramping, and safety interlocks for reproducible processing.

Applications

Application Description Key Benefit
Perovskite Solar Cell Fabrication Deposition of top metal contacts (Au, Ag, Al), electron/hole transport layers, and halide precursors directly inside an inert glove box environment. Eliminates moisture-induced phase degradation and pinhole formation, ensuring high power conversion efficiency and extended operational stability.
OLED & PLED Display Development Evaporation of small-molecule organic emissive layers, charge injection layers, and low-work-function cathode metals without air exposure. Prevents organic layer oxidation and quenching centers, resulting in superior luminance, uniform pixel output, and prolonged device lifespan.
Semiconductor & Microelectronics R&D Synthesis of high-purity metal contacts, interconnects, barrier layers, and semiconductor thin films on silicon, quartz, and flexible substrates. Delivers atomically smooth interfaces, minimal defect densities, and precise film stoichiometry under ultra-clean vacuum conditions.
Functional Dielectric & Optical Coatings Sputtering and thermal deposition of optical interference filters, anti-reflective coatings, passivation oxides, and high-k dielectric thin films. Ensures uniform refractive index, tight thickness tolerance, and low scattering losses across large-area substrates.
Advanced Sensor & Transducer Fabrication Growth of gas-sensing functional films, piezoelectric thin layers, magnetic sensor stacks, and bio-compatible transducer coatings. Enhances signal-to-noise ratios and transducer sensitivity through ultra-clean layer interfaces and repeatable microstructural morphology.
Superconducting & Magnetic Thin Films Precise sputtering of transition metals, rare-earth alloys, and superconducting layered compounds under controlled process atmospheres. Maintains sharp magnetic domain boundaries and high critical transition temperatures without atmospheric impurity contamination.
Device Encapsulation & Packaging Application of barrier coatings, UV-curable epoxy seals, and cover glass attachment directly within the glove box following thin film growth. Completes end-to-end device fabrication in a unified envelope, preventing moisture ingress prior to final exterior testing.

Technical Specifications

System Parameter ST16 Base Specification ST16 Advanced Sputtering / Co-Evaporation Configuration
Base Vacuum Level ≤ 5.0 × 10⁻⁴ Pa (Chamber pre-evacuated) ≤ 8.0 × 10⁻⁵ Pa (Bakeout enabled)
Glove Box Atmosphere Purity H2O < 1 ppm, O2 < 1 ppm H2O < 0.1 ppm, O2 < 0.1 ppm
Glove Box Gas Working Medium High-purity Nitrogen (N2) / Argon (Ar) High-purity Argon (Ar) / Nitrogen (N2) / Helium (He)
Glove Box Leak Rate < 0.001 vol%/h < 0.001 vol%/h
Chamber Structure Material SUS304 Austenitic Stainless Steel, Electropolished SUS304 / SUS316L Stainless Steel, High-Vacuum Mirror Finish
Deposition Source Configuration 4 × Thermal Resistance Evaporation Boats / Crucibles 4–6 × Thermal Sources + 2–3 × Magnetron Sputtering Guns (DC/RF)
Substrate Holder Size Up to 100 mm diameter (or customized multi-wafer) Up to 200 mm diameter (or customized matrix carrier)
Substrate Motion & Rotation 0 to 30 RPM continuously adjustable 0 to 50 RPM reversible with motorized height adjustment
Substrate Heating Range Ambient to 300°C (±1°C PID control) Ambient to 500°C / 800°C (Radiant / Ceramic heater, ±0.5°C)
Film Thickness Monitoring Single/Dual Quartz Crystal Monitor (Resolution 0.1 Å) Multi-channel QCM with automated rate control & tooling factor calibration
Vacuum Pumping Architecture Molecular Turbopump + Rotary Vane / Dry Scroll Pump High-speed Magnetic Levitation Turbopump + Oil-Free Scroll Roughing Pump
Glove Box Antechamber Dimensions Main: Φ360 mm × L600 mm; Mini: Φ150 mm × L300 mm Main: Φ400 mm × L600 mm; Mini: Φ150 mm × L330 mm with auto-vacuum
Power Supply Compatibility 220V AC / 380V AC, 3-Phase, 50/60 Hz 380V AC, 3-Phase, 50/60 Hz, 15–25 kW
Control Architecture Central PLC + Industrial Color Touchscreen HMI Integrated PC / PLC System with Data Logging & Recipe Management

Why Choose This Product

  • Integrated Process Continuity: By housing the entire thin film growth, substrate preparation, and encapsulation workflow within a unified ultra-pure envelope, this system eliminates transfer-induced oxidation and particulate defects, driving significant increases in device yield.
  • Precision Engineering and Film Uniformity: Engineered substrate stages, optimized source-to-substrate throw distances, and precision quartz crystal rate controllers provide sub-angstrom deposition control, ensuring exceptional batch-to-batch repeatability.
  • Versatile Multi-Material Capability: Accommodates a comprehensive range of material classes—from sensitive organic molecules and low-melting metals to refractory targets, transparent oxides, and functional dielectrics—in thermal evaporation and sputtering configurations.
  • Robust Safety and Interlock Architecture: Built with multi-tier hardware and software interlocks covering vacuum levels, water cooling flow, gas overpressure, and heater temperatures to safeguard both user and valuable research substrates.
  • Customizable Modular Architecture: The platform offers adaptable glove box dimensions, multiple deposition head combinations, customized substrate masking fixtures, and integrated in-situ measurement tools tailored to specific research programs.

Contact our technical engineering team today to configure a custom glove box integrated vacuum deposition system optimized for your specific thin film and optoelectronic research requirements.

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Glove Box Integrated Vacuum Coating System for Advanced Thin Film Deposition

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