Glove Box
Single Station Laboratory Glovebox with Standalone Gas Purification Cabinet for Inert Atmosphere Research
Item Number : ST07
Price varies based on specs and customizations
- Purification Performance
- H2O < 1 ppm, O2 < 1 ppm
- Internal Working Dimensions
- 1220 mm (L) × 750 mm (D) × 900 mm (H)
- Gas Circulation Rate
- 90 m³/h with Variable Frequency Control
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Product Overview
This high-purity single-station laboratory glove box system provides an ultra-clean, controlled inert atmosphere engineered specifically for sensitive electrochemical research and advanced materials synthesis. Featuring an integrated standalone gas purification cabinet located beneath the primary workstation, the equipment maintains strict moisture and oxygen levels below 1 ppm. The closed-loop gas circulation architecture utilizes automated regeneration sequences to deliver long-term atmospheric stability under high-throughput testing conditions.
Designed primarily for next-generation lithium battery prototyping, organometallic chemistry, perovskite solar cell fabrication, and semiconductor processing, this system shields sensitive compounds from atmospheric oxidation and moisture degradation. Operators conduct delicate manipulations through an ergonomically angled viewing window equipped with high-durability butyl gloves. Dual integrated antechambers provide rapid, contamination-free sample ingress and egress without compromising internal atmospheric purity.
Constructed from heavy-gauge 304 stainless steel with oil-brushed internal surfaces, this unit delivers exceptional mechanical rigidity, chemical resistance, and hermetic sealing integrity. Controlled by an intuitive Siemens programmable logic controller (PLC) and smart touchscreen interface, the system automates chamber pressure regulation, antechamber evacuation cycles, and purge protocols. Precision gas sensors and premium international sub-components guarantee continuous reliability during mission-critical research and development workflows.
Key Features
- Ultra-Pure Atmospheric Control: Closed-loop gas purification driven by high-capacity copper catalyst and molecular sieve beds maintains both moisture and oxygen concentrations below 1 ppm under standard operating conditions.
- Independent Standalone Purification Cabinet: Dedicated cabinet architecture positioned beneath the main enclosure optimizes airflow routing, simplifies routine maintenance access, and accommodates high-capacity purification media.
- Automated Catalyst Regeneration: Fully automated PLC-controlled thermal regeneration sequence restores catalyst efficiency without requiring hardware disassembly, utilizing standard nitrogen/argon-hydrogen mixtures.
- Dual Modular Antechambers: Large cylindrical antechamber with sliding tray handles bulk hardware, while a secondary compact antechamber accelerates rapid tool and sample transfer to minimize gas consumption.
- Precision PLC and Touchscreen Interface: Centralized Siemens control system manages box pressure, real-time oxygen/moisture telemetry, automated purge sequences, and includes auto-lockout password security.
- Robust Integrated Manifold Block: Custom stainless steel valve seat integrates six solenoid operations into a single block, drastically minimizing external tubing, potential leak paths, and maintenance overhead.
- Dynamic Pressure Management: Adaptive digital pressure monitoring automatically regulates chamber pressure within a customizable +/-10 mbar range, backed by a +/-12 mbar high-limit protective interlock and foot pedal override.
- Rejuvenable Moisture and Zirconia Oxygen Sensors: High-accuracy analytical sensors deliver continuous 0–500 ppm H2O and 0–1000 ppm O2 tracking, featuring cleanable, solvent-tolerant sensor heads built for long industrial lifespans.
- Integrated Solvent Vapor Trapping: Internal solvent adsorber loaded with activated carbon captures volatile organic compounds before they can poison catalytic purification beds or degrade butyl gloves.
- Ergonomic Stainless Steel Enclosure: Heavy-duty 3 mm 304 stainless steel body features an 8 mm tempered safety glass front window, adjustable shelving, internal power feedthroughs, and sealed KF40 utility flanges.
Applications
| Application | Description | Key Benefit |
|---|---|---|
| Lithium-Ion Battery Assembly | Prototyping coin, pouch, and cylindrical cells with moisture-reactive electrolytes and lithium metal anodes. | Prevents violent electrolyte hydrolysis and surface passivation, ensuring reproducible electrochemical performance. |
| Solid-State Electrolyte Synthesis | Processing sensitive sulfide, halide, and oxide ceramic solid electrolyte powders under pure argon. | Eliminates hazardous H2S gas evolution and preserves ionic conductivity across reactive solid-state interfaces. |
| Organometallic & Catalysis Chemistry | Handling pyrophoric reagents, Grignard reagents, metal hydrides, and moisture-sensitive transition metal catalysts. | Guarantees worker safety while preserving catalytic activity and preventing premature reaction quenching. |
| Perovskite Optoelectronics | Spin-coating and thermal annealing of lead halide perovskite precursor films for photovoltaic cells. | Halts moisture-induced degradation during crystallization, directly improving device power conversion efficiency. |
| Inert Powder Metallurgy & 3D Printing | Post-processing, sieving, and packaging fine titanium, aluminum, and nickel superalloy powders. | Eliminates oxide film formation, ensuring optimal powder flowability, density, and sinterability in additive manufacturing. |
| Specialty OLED & Semiconductor Packaging | Encapsulating organic light-emitting diodes, quantum dots, and delicate microelectronic junctions. | Shields active organic layers from ambient moisture and oxygen ingress to prevent non-radiative dark spot formation. |
| Nuclear & Hazardous Isotope Handling | Containing radioactive or toxic samples under strictly regulated negative/positive pressure cascades. | Provides hermetic containment with certified HEPA/dust particulate filtration down to 0.3 microns. |
Technical Specifications
| Specification Category | Parameter | Specification Value (Item No. ST07) |
|---|---|---|
| Model Identification | Product Item Number | ST07 |
| System Architecture | Glove Station Configuration | Single Station, 2 Glove Ports, Ergonomically Tilted Window |
| Purification Unit Location | Standalone purification cabinet beneath main chamber | |
| Control Architecture | Siemens PLC with high-resolution color touchscreen interface | |
| Atmospheric Purity | Target Moisture Level (H2O) | < 1 ppm (Standard Conditions: 20°C, 1 atm, 99.999% inert gas) |
| Target Oxygen Level (O2) | < 1 ppm (Standard Conditions: 20°C, 1 atm, 99.999% inert gas) | |
| Main Chamber Body | Chamber Construction Material | 304 Stainless Steel, Acid-Resistant, 3 mm Wall Thickness |
| Internal Dimensions (L × D × H) | 1220 mm × 750 mm × 900 mm | |
| Internal Surface Treatment | Oil-film brushed stainless steel finish | |
| External Surface Treatment | High-durability powder-coated industrial finish (Signal White) | |
| Viewing Window Panel | Transparent Tempered Safety Glass, 8 mm Thickness, Angled | |
| Glove Ports | High-strength Aluminum, O-ring sealed, self-lubricating seal | |
| Gloves Specification | Butyl Rubber, 8" Port Diameter, 32" Length, Thickness ≥ 0.4 mm | |
| Internal Dust Filtration | 0.3 μm particulate filters on gas inlet and gas outlet ports | |
| Shelving Unit | Adjustable 2-tier 304 stainless steel interior shelving | |
| Internal Illumination | Integrated forward-mounted LED lighting above front window | |
| Standard Feedthroughs | 3 × DN 40 KF blind flanges, 1 × Internal 220V power socket | |
| Large Antechamber | Antechamber Dimensions | Diameter: 360 mm, Length: 600 mm (Right-side mounted) |
| Material & Sliding Mechanism | 304 Stainless Steel chamber with 304 Stainless Steel sliding tray | |
| Chamber Doors | Dual 10 mm thick anodized aluminum vertical lifting doors | |
| Evacuation & Refill Control | Automated solenoid operation via touchscreen; analog pressure gauge | |
| Small Antechamber | Antechamber Dimensions | Diameter: 150 mm, Length: 300 mm (100 mm internal projection) |
| Chamber Connection Type | Modular flanged connection (non-welded, expandable) | |
| Chamber Doors & Tray | Dual flip-latch doors, 304 stainless steel sliding tray | |
| Evacuation & Refill Control | Automated solenoid operation via touchscreen; analog pressure gauge | |
| Gas Purification System | Purification Column Type | Single-column, 304 Stainless Steel containment vessel |
| Purification Reactants | 5 kg Copper Catalyst (Deoxygenation), 5 kg Molecular Sieve (Moisture) | |
| Purification Capacity | Deoxygenation: 60 L O2 capacity; Moisture removal: 2 kg H2O capacity | |
| Working Inert Gases | High-purity Nitrogen (N2), Argon (Ar), or Helium (He) | |
| Circulation Blower | Variable frequency blower, max flow capacity 90 m³/h | |
| Catalyst Regeneration | Automated PLC cycle using 5–10% H2 in inert balance gas | |
| Integrated Valve Assembly | Custom 6-valve integrated 304 stainless steel manifold block | |
| Main Isolation Valves | DN 40 KF electro-pneumatic angle valves | |
| Vacuum System | Rotary Vane Vacuum Pump | Dual-stage rotary vane pump, 12 m³/h displacement |
| Ultimate Vacuum Rating | ≤ 2 × 10⁻¹ Pa (0.002 mbar) | |
| Pump Accessories | Oil mist exhaust filter and gas ballast control valve | |
| Pressure Regulation | Working Chamber Setpoint | Programmable within +/- 10 mbar nominal working window |
| Overpressure Protection | Automatic safety interlock triggered when exceeding +/- 12 mbar | |
| Auxiliary Pressure Control | Bi-directional foot pedal switch for hands-free box pressure tuning | |
| Analytical Sensors | Moisture Analyzer | Range: 0–500 ppm; renewable/washable probe technology |
| Oxygen Analyzer | Range: 0–1000 ppm; solid-state Zirconia (ZrO2) sensor cell | |
| Solvent Trap Unit | Organic Solvent Adsorber | Internal canister (Ø 136 mm × 256 mm H) loaded with 2 kg activated carbon |
Why Choose This Product
- Engineered Gas Tightness: Advanced integrated manifold design eliminates excessive pipe threads and flexible hoses, minimizing leak rates and guaranteeing stable sub-ppm operation over multi-year research campaigns.
- Industrial Grade Component Sourcing: Built exclusively with globally recognized vacuum pumps, high-precision German pressure sensors, premium valves, and certified Siemens microelectronics for uncompromised uptime.
- Superior Chemical & Solvent Resilience: Heavy acid-resistant 304 stainless steel, robust butyl gloves, regenerable sensor probes, and dedicated vapor traps ensure complete compatibility with harsh organic solvents and corrosive battery chemistries.
- Flexible Laboratory Integration: Modular antechambers, expandable KF40 feedthrough ports, and a compact standalone lower purification cabinet fit standard laboratory footprints without sacrificing internal working volume.
- Long-Term Operational Economy: Fully regenerable molecular sieves, cleanable moisture sensors, and robust zirconia oxygen cells lower consumable expenses and dramatically reduce total cost of ownership.
Contact our technical engineering team today to request a detailed quotation, discuss custom chamber dimensions, or integrate specialized analytical feedthroughs for your laboratory workflow.
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