Glove Box
Single Station Single Sided Glove Box Inert Gas Purification Workstation
Item Number : ST04
Price varies based on specs and customizations
- Atmospheric Purity
- < 1 ppm (H2O and O2)
- Chamber Leak Rate
- ≤ 0.05 vol%/h
- Circulation Blower Flow Rate
- 90 m³/h
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Product Overview
This single station single sided glove box provides an uncompromising hermetic environment engineered for sensitive electrochemical synthesis, advanced battery assembly, and moisture-critical materials processing. Built with an acid-resistant 304 stainless steel enclosure and an advanced closed-loop gas circulation architecture, this system maintains both moisture and oxygen concentrations below 1 ppm under standard operating conditions. By continuously scrubbing ambient impurities, the equipment establishes a reliable baseline for repeatable scientific research and high-yield pilot production.
Designed for modern research facilities, the workstation accommodates complex workflows spanning lithium-ion and sodium-ion battery fabrication, solid-state electrolyte synthesis, organometallic chemistry, and perovskite photovoltaic handling. Ergonomic features such as an inclined safety glass viewing window, dual transition antechambers, and bidirectional foot-pedal pressure controls allow operators to transfer materials and manipulate delicate instrumentation with maximum precision and zero atmospheric contamination.
Industrial-grade components ensure long-term mechanical stability and continuous operational uptime. With integrated solvent vapor adsorption, hydrofluoric acid removal traps, and automated programmable regeneration cycles, this system delivers dependable environmental stability even during prolonged experimental protocols involving volatile reagents.
Key Features
- Sub-PPM Atmospheric Purity: Integrated single-column purification unit loaded with high-efficiency BASF copper catalyst and UOP molecular sieves continuously reduces both moisture (H2O) and oxygen (O2) levels to below 1 ppm.
- Automated Siemens PLC Management: High-resolution touchscreen interface delivers centralized automation for pressure regulation, automated chamber purging, multi-stage catalyst regeneration, and real-time self-diagnostic monitoring.
- Dual Transition Antechamber Architecture: Equipped with a large motorized vacuum antechamber (Ø360 mm × 600 mm) featuring vertical lifting doors and a compact mini-antechamber (Ø150 mm × 300 mm) for rapid sample throughput with minimal purge gas loss.
- Robust Acid-Resistant Enclosure: Constructed from heavy-duty 3 mm thick 304 stainless steel with a clean-finished interior, paired with an 8 mm laminated tempered safety glass window for superior chemical resilience and operator visibility.
- Dynamic Chamber Pressure Regulation: Halstrup pressure sensing technology maintains chamber pressure within an adjustable ±10 mbar operating window, supported by automatic safety cutoffs at ±12 mbar and hands-free foot pedal adjustment.
- Specialized Gas Purification & Trapping: Standard dual-filter configuration includes a 9 kg activated carbon organic solvent adsorber and a 9 kg activated alumina hydrofluoric acid (HF) trap to protect internal catalysts from volatile chemical degradation.
- Continuous Analytical Precision: Embedded VTI electrochemical analyzers provide real-time monitoring of oxygen via a durable zirconia (ZrO2) sensor and moisture through a regenerable, cleanable P2O5 platinum electrode sensor.
- High-Capacity Closed-Loop Circulation: High-performance Dargang blower circulates inert gas at rates up to 90 m³/h through 0.3 μm particulate filters, ensuring rapid equilibrium and homogeneous gas distribution throughout the chamber.
Applications
| Application | Description | Key Benefit |
|---|---|---|
| Lithium & Sodium Battery Assembly | Assembly of coin cells, pouch cells, and split test cells involving metallic lithium, sodium foils, and reactive liquid electrolytes. | Prevents rapid oxidation and moisture degradation, ensuring accurate electrochemical impedance and cycling performance data. |
| Solid-State Electrolyte Research | Synthesis, cold pressing, and hermetic encapsulation of sulfide-, oxide-, and polymer-based solid electrolyte powders. | Eliminates hydrolysis reactions that generate toxic H2S gas and compromise ionic conductivity. |
| Perovskite Solar Cell Fabrication | Spin-coating, thermal annealing, and encapsulation of organic-inorganic hybrid metal halide perovskite precursor films. | Protects moisture-sensitive perovskite crystallites during formation, boosting photovoltaic conversion efficiency and film uniformity. |
| Organometallic & Catalytic Synthesis | Manipulation, purification, and storage of pyrophoric reagents, Grignard reagents, and sensitive transition-metal catalysts. | Guarantees an inert nitrogen or argon environment, preventing spontaneous combustion and loss of catalytic activity. |
| Supercapacitor & Energy Storage R&D | Electrolyte filling, electrode wetting, and final sealing of ultra-capacitor cores with sensitive non-aqueous solvents. | Maintains low volatile organic background and strict dryness to achieve maximum working voltage and extended cycle life. |
| Specialized Metallurgy & Laser Sealing | Inert handling of fine reactive metal powders (titanium, zirconium) and micro-welding of hermetic electronic packages. | Minimizes gas entrapment, porosity, and oxide inclusions in finished welds and sintered components. |
Technical Specifications
| System Category | Parameter Specification | Value / Detail (ST04) |
|---|---|---|
| Model Identification | Product Item Number | ST04 |
| Core Performance | Moisture Level (H2O) | < 1 ppm (Standard condition: 20°C, 1 atm, 99.999% inert gas) |
| Oxygen Level (O2) | < 1 ppm (Standard condition: 20°C, 1 atm, 99.999% inert gas) | |
| Overall Leak Rate | ≤ 0.05 vol%/h | |
| Main Enclosure | Internal Dimensions (L × D × H) | 1220 mm × 750 mm × 900 mm |
| Box Material | 304 Stainless Steel, 3.0 mm thickness, acid-resistant | |
| Exterior / Interior Finish | White powder-coated exterior / Natural stainless steel interior | |
| Viewing Window | 8 mm inclined tempered safety glass with protective film | |
| Glove Ports | Machined aluminum alloy, O-ring sealed, 2 ports | |
| Glove Specifications | Ansell Butyl Rubber, 0.4 mm thickness, 8" diameter, 32" length | |
| Internal Shelving | Multi-tier height-adjustable 304 stainless steel rack | |
| Internal Lighting | High-intensity glare-free LED strip mounted above front window | |
| Feedthrough Ports | 3 × DN40 KF spare blind flanges (customizable); 1 × 220V power port (1.2 kW) | |
| Large Antechamber | Dimensions | Diameter 360 mm, Length 600 mm (Right-side mounted) |
| Material & Finish | 304 Stainless Steel, polished interior / white painted exterior | |
| Door & Tray Mechanism | Dual 10 mm anodized aluminum vertical sliding doors; 304 SS sliding tray | |
| Control & Pressure Display | PLC touchscreen automated solenoid valve control; analog pressure gauge | |
| Small Antechamber | Dimensions | Diameter 150 mm, Length 300 mm (100 mm extension into main chamber) |
| Material & Finish | 304 Stainless Steel, brushed interior / white painted exterior | |
| Door & Mechanism | Dual quick-clamp compression doors; integrated sliding tray | |
| Control & Pressure Display | Manual 3-way ball valve; analog pressure gauge | |
| Gas Purification System | Purification Column | Single-column 304 stainless steel vessel |
| Catalytic Filling | 5 kg BASF Copper Catalyst (Deoxygenation) + 5 kg UOP Molecular Sieve (Desiccation) | |
| Purification Capacity | Oxygen removal: 60 L; Water absorption: 2.0 kg | |
| Compatible Working Gases | Nitrogen (N2), Argon (Ar), Helium (He) | |
| Blower Circulation Flow | Integrated Dargang blower, 90 m³/h flow capacity | |
| Particulate Filtration | Dual 0.3 μm HEPA filters (1 gas inlet, 1 gas outlet) | |
| Regeneration Process | Automated PLC programmed cycle using working gas with 5–10% H2 mixture | |
| Vacuum System | Vacuum Pump Type | Edwards rotary vane pump with oil mist filter and gas ballast |
| Displacement Speed | 12 m³/h rated displacement (8 m³/h effective working throughput) | |
| Ultimate Vacuum Level | ≤ 2.0 × 10⁻¹ Pa | |
| Control & Instrumentation | Automation Hardware | Siemens PLC controller with color touch HMI screen |
| Pressure Regulation Range | Operating pressure configurable within ±10 mbar; safety trip at ±12 mbar | |
| Hands-Free Control | Bidirectional pneumatic foot pedal for pressure increase/decrease | |
| Differential Pressure Sensor | Halstrup high-precision pressure sensor (Germany) | |
| Primary Dial Gauges | WIKA mechanical pressure gauges (Germany) | |
| Moisture Sensor (H2O) | VTI P2O5 platinum electrode analyzer, range 0–500 ppm (cleanable/renewable) | |
| Oxygen Sensor (O2) | VTI Zirconia (ZrO2) solid electrolyte analyzer, range 0–1000 ppm | |
| Process Valves & Fittings | Burket electromagnetic solenoid valves; Legris pneumatic fittings | |
| Auxiliary Traps | Solvent Adsorption Unit | Ø237 mm × 407 mm (304 SS), 9 kg activated carbon with manual isolation valves |
| Hydrofluoric Acid (HF) Trap | Ø237 mm × 407 mm (304 SS), 9 kg activated alumina with manual isolation valves |
Why Choose This Product
- Tier-One Component Engineering: Built exclusively with world-class sub-assemblies—including Edwards vacuum pumps, Siemens PLC controllers, BASF catalysts, and Burket valves—ensuring minimal maintenance overhead and decades of operational longevity.
- Renewable Sensor & Purification Technology: The VTI moisture analyzer features a regenerable P2O5 sensor design that can be washed and recalibrated on-site, eliminating costly sensor replacements caused by accidental solvent exposure.
- Dual Volatile Trapping Systems: Standard inclusion of dedicated 9 kg organic solvent and HF traps safeguards internal catalytic columns, extending catalyst life and reducing regeneration frequency in battery electrolyte workflows.
- Turnkey Integration & Ergonomics: From hands-free foot-pedal pressure controls to integrated LED lighting and adjustable multi-tier shelving, every mechanical interface is optimized for continuous operator comfort and streamlined sample transfer.
- Comprehensive Factory Acceptance Testing: Each unit undergoes stringent helium leak testing and atmospheric verification before dispatch to guarantee baseline water and oxygen readings strictly below 1 ppm.
Contact our technical engineering team today to request a detailed quotation, discuss custom chamber dimensions, or integrate tailored feedthrough interfaces for your specific laboratory research requirements.
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